Well, that's the thing.
Within the procedures manual it was clearly stated that we had to weigh first, then dissolve, and that pretty much seals the deal to make me think this isn't a trick question.\
Besides, the question was formulated as a "Why must you weight before mixing" instead of a "Must you weight before mixing", kind of implies there is not room of argument about this point.
I can't really prove right or wrong because I didn't specifically weight and record the before and after mixing weights, but come on, that's common sense.
Just because it's dissolved it doesn't become lighter.