TiI4

You can use batteries bell-type for get zinc and reacting zinc with sulfuric acid then make the electrolysis of ZnSO4. sodium hydroxide is hard to make but you can get from crystal drain cleaner. look at the link: http://www.youtube.c.../56/knc1lSupAwQ

be watching the comments, I think I'll do a test in a test tube filled with chlorine , the gas formed will condense in another test tube, the gas that will not be condensing (chlorine CO2 and a bit of TiCl4) will be dissolved in water is 3-5 degrees Celsius because TiCl4 reacts violently with the water has a temperature of 15 degrees Celsius and higher.

I wanted to do this reaction with a type of test tube under an atmosphere of chlorine under pressure (because of the production of chlorine, which is produced in an Erlenmeyer flask) at 900 degree Celsius and condensing the gas into another test tube which has at -20 degrees Celsius. I know the hazard of chlorine, titanium dioxide and TiCl4.

I want to Syntesis TiCl4, here I find this reaction: TiO2 + 2Cl2 + C > TiCl4 + CO2 I know that this reaction occurs around 900 degree celcius. If you think that this reaction is possible with borosilicate glassware please tell my. 30122929-Titanium-Compounds-Inorganic.pdf