Sedit
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Hey I just got your message, sorry its been sometime since I signed in. Mixing H2SO4 with NaOAc in equal molar ratios creates acetic acid and sodium sulfate. Its simple distillation at that point but it tends to burn the AcOH. I have found a new means of extracting the Acetic acid very clean and quick using Dichloromethane and If you look over at science madness you can find some comments I made.
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Hi Sedit
I read your comment about having distilled conc. acetic acid with sulfuric and sodium acetate anhydrous. Can u tell me a little more info. First, do you have any notes on the whole procedure or know where I can get it. second, how long does it take for finish the distillation. third, at what temp is the distillate coming over to the receiving flask. thanks.