DFC

HI Knumbnuts, Thanks a lot for your reply, which base you recommned to use if I use THF or ETOH as solvent?, at catalytic o stoichiometry? Do you think temperature will improve? thanks D

Dear all, I am trying to make this compond ( attached) and I am not getting anywhere. I have done the reaction by Dropwise addition of boc-protected hydrazine to 1,3-diiodopropane at RT using ACN as solvent and a catalytic base ( NaHCO3). Can you recommend any other reaction media? Suggestions? Reaction.pdf