jdurg Posted September 2, 2005 Posted September 2, 2005 Hey guys. This past week I had some free time and decided to make some sodium iodide from my extra sodium metal and iodine. I photographed the entire experiment and have written an article for it at a website I help run. I thought I'd mention it to you guys here since we seem to have a lot of people here who like to do little experiments like this every now and then. The article can be found at this link which is the website I work at.
Silencer Posted September 2, 2005 Posted September 2, 2005 You switch from first to third person a lot. Neat experiment, though.
woelen Posted September 2, 2005 Posted September 2, 2005 This is fun! What is remarkable is that in the second experiment in the new vial, you did not get copious amounts of I2-vapor. I have done such an experiment with magnesium and iodine. I also want to try with calcium and iodine. I have 75 grams of pea-sized granules of Ca-metal, so this experiment should be possible quite well with the little granules. The latter may be more dangerous, so I have to think carefully about how to do this. The Mg/I2 reaction was initiated by water, can the calcium reaction also be initiated with water?
budullewraagh Posted September 2, 2005 Posted September 2, 2005 i think that the calcium would react rather quickly with the water, so you'll end up with a whole lot of calcium hydroxide.
jdurg Posted September 3, 2005 Author Posted September 3, 2005 You switch from first to third person a lot. Neat experiment' date=' though.[/quote'] Thank you. Yeah, I'm a science person and writing is just a byproduct of mine. I was just writing what went through my head. The experiment was fun, however. In the initial vial, I had a LOT more iodine vapor in there, yet a lot of it leaked out when the vial cracked so a good deal of the iodine was lost. In the second vial, I decided to just add the iodine slowly to the hot/molten sodium. That worked a LOT better and resulted in less iodine vapor. I was happy to see that most of the sodium reacted with the iodine and not the occasional drop of water I put in there to accelerate the reaction. It didn't take much vinegar at all to neutralize the final solution.
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