dom3mo Posted December 30, 2007 Posted December 30, 2007 I am wondering can you make a chlorate by electrolysis of the hypochlorite.
Melvin Posted December 31, 2007 Posted December 31, 2007 Actually, you don't need the hypochlorite. You can just use the chloride (aka sodium chloride, table salt). Place two platinum electrodes inside a cup of salt water and apply electricity. Hydrogen will come off the negative electrode.
dom3mo Posted December 31, 2007 Author Posted December 31, 2007 I was juke wondering if the hypochlorite would work because it would not make chloride thus making the purification step easier.
YT2095 Posted December 31, 2007 Posted December 31, 2007 well unless you plan on doing Gallons of this you will only end up with at best a few grams per liter! the stuff is only 5% in fact the Strongest Possible NaOCl soln is a mere 12%.
Melvin Posted December 31, 2007 Posted December 31, 2007 The chloride is not formed. You put the chloride in to get the chlorate. The electrolysis converts the chloride to the chlorate. If I remember correctly, the reaction is: 3H2O + NaCl --> 3H2 + NaClO3.
YT2095 Posted December 31, 2007 Posted December 31, 2007 and don`t forget to add a little Potassium dichromate to stop back reduction. what do you want the stuff for anyway?
dom3mo Posted December 31, 2007 Author Posted December 31, 2007 Ok I think I made it ill try a test when get some HS204.
Melvin Posted December 31, 2007 Posted December 31, 2007 Why are you waiting until you get H2SO4? You need K2Cr2O7, NaCl, H2O, and electricity!
Fable Posted January 1, 2008 Posted January 1, 2008 maybe he thought of elektrolysis as in "car battery".
Fuzzwood Posted January 1, 2008 Posted January 1, 2008 Dude, please buy a book first, then try to experiment. I guess it was meant for new year for being cool when his hands are blown off.
YT2095 Posted January 1, 2008 Posted January 1, 2008 agreed, I also suspect the intentions of this user looking at his other posts too. there`s also Nothing in here that hasn`t been covered (Ad Nauseum) elsewhere on this site too. ergo.... Thread Closed.
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