sk530 Posted May 1, 2008 Posted May 1, 2008 I need to make the acetal of a polyol but I'm limited to NMP (or DMF or DMSO) as a solvent. I was planning on using methane sulfonic acid as the catalyst, but I'm wondering if the acid will just protonate the amide solvent. Any suggestions?
Tartaglia Posted May 15, 2008 Posted May 15, 2008 Use benzene, p-toluenesulphonic acid and azeotrope the water out with a dienstark apparatus
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