gaidzag Posted July 11, 2014 Posted July 11, 2014 I received a treasure trove of glassware from a chem professor friend who found them in the dumpster of the chem building on his way out from work. Most of the stuff I recognize, but there are a few pieces that I've never seen and can't find on google and that even he doesn't know what they are. I'm hoping someone here can help. Here's the first piece. It's stuck to the top of a Vigreux column. Does anyone know what it's called and what its purpose is?
studiot Posted July 11, 2014 Posted July 11, 2014 (edited) Looks like part of a reflux condenser to me. http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322002000100009 Edited July 11, 2014 by studiot
gaidzag Posted July 12, 2014 Author Posted July 12, 2014 Thanks, studiot, for the quick reply. I should have been more specific--I figure it's part of a distillation apparatus, but I have not been able to find this specific piece in any literature. Even the diagram in the article you referred me to doesn't have quite this piece in it.
Elite Engineer Posted July 12, 2014 Posted July 12, 2014 I was going to say a steam distillation apparatus, but you could have fooled me.
John Cuthber Posted July 12, 2014 Posted July 12, 2014 (edited) I think it's a variation on one of these http://www.scientificglass.co.uk/contents/en-uk/d68_Distillation_Heads,_Splash.html it's purpose is to trap spray in the vapour and return it to the distilling flask so you get less impurities carried over into the product. Incidentally, it's probably pointless on to of a fractionating column. Edited July 12, 2014 by John Cuthber
gaidzag Posted July 13, 2014 Author Posted July 13, 2014 Thanks, John. I think you're right on both counts. And not only is it useless on the fractionating column, it's stuck there!
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