lux94 Posted November 7, 2015 Posted November 7, 2015 Hello, So by a mistake, I mixed contents of two flasks together and contaminated my pure product (salt) with sulfonyl amide.I'd like to get some advice on how I could separate them.Could I extract amine salt from organic phase with water, and if so, what could be the right conditions (like pH) for the salt to dissolve in water?I'm also adding picture of molecule structures.
hypervalent_iodine Posted November 8, 2015 Posted November 8, 2015 Do you have a good idea of what organic solvents the sulfonamide is soluble in? I doubt the salt is soluble in many organic solvents, so if you remove whatever solvent they are currently in, you should simply be able to wash the sulfonamide through a frit or with gravity filtration.
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